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Org. The product is recrystallized from a methylene chloride-methanol mixture to yield 682 mg of 6α,9α- difluoroprednisolone 17α,21-methylorthobutyrate, also identified as 17α,21- (1'-methoxy)-n-butylidenedioxy-6α,9α-difluoro-δ1,4-pregnadiene-11β-ol-3,20- dione.
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